N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid

Base Information

• Chemical Name: N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid
• CAS No.: 118560-99-9
• Molecular Formula: C₃₈H₂₉NO₅
• Molecular Weight: 579.652

Synonyms:N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid

Chemical Property of N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid

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Technology Process of N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid

There total 1 articles about N¹-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

N,N'-bis(2,5-di-tert-butylphenyl)perylene-3,4:9,10-bis(dicarboximide) (83054-80-2,99571-55-8,99571-56-9,121468-40-4,121470-76-6) → N1-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid (118560-99-9)

Guidance literature:

With potassium hydroxide; In tert-butyl alcohol; Heating;

Reference yield: 84.0%

N1-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid (118560-99-9) + p-aminoiodobenzene (540-37-4) → N-(4-Iodophenyl)-N'-(2,5-di-tert-butylphenyl)-3,4,9,10-perylenebis(dicarboximide) (359857-37-7)

Guidance literature:

With 1H-imidazole; zinc diacetate; at 130 ℃; for 1h;

DOI:10.1021/jp010335i

Reference yield: 64.0%

4-iodobenzyl amine (39959-59-6) + N1-(2,5-Di-tert-butylphenyl)-3,4,9,10-perylentetracarbonsaeure-3,4-anhydrid-9,10-imid (118560-99-9) → N-(4-iodobenzyl)-N’-(2,5-di-tert-butylphenyl)perylene-3,4,9,10-tetracarboxylic acid bisimide

Guidance literature:

With 1H-imidazole; at 140 ℃; for 4h; Inert atmosphere;

DOI:10.1002/chem.201201661

upstream raw materials:

N,N'-bis(2,5-di-tert-butylphenyl)perylene-3,4:9,10-bis(dicarboximide)

Downstream raw materials:

N-(4-Iodophenyl)-N'-(2,5-di-tert-butylphenyl)-3,4,9,10-perylenebis(dicarboximide)

N-(2',5'-di-tert-butylphenyl)-N'-(3',4'-dicyanophenyl)perylene-3,4:9,10-bis(carboximide)

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