2Mn^IVTPP

Base Information

• Chemical Name: 2Mn^IVTPP
• CAS No.: 85282-35-5
• Molecular Formula: C₆₀H₄₄I₂MnN₄O₆
• Molecular Weight: 1225.78
• Mol file: 85282-35-5.mol

Synonyms:2Mn^IVTPP

Chemical Property of 2Mn^IVTPP

Chemical Property:

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Technology Process of 2Mn^IVTPP

There total 1 articles about 2Mn^IVTPP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(acetato)(5,10,15,20-tetraphenylporphyrinato)manganese(III) + iodosylbenzene (536-80-1) → 2MnIVTPP (85282-35-5)

Guidance literature:

With glacial acetic acid; In chlorobenzene; Mn-compound dissolved in chlorobenzene, oxidized in presence of glacialacetic acid with a slight excess of iodosylbenzene; filtered into a receiver cooled to -35°C, hexane added to stirred chilled soln., recrystd. from CCl4/hexane at -30°C; elem. anal.;

DOI:10.1021/ja00347a079

upstream raw materials:

iodosylbenzene