4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Base Information

Chemical Name:4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether
CAS No.:191331-97-2
Molecular Formula:C₁₄H₂₀O₄
Molecular Weight:252.31
Hs Code.:

Synonyms:4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Chemical Property of 4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

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Technology Process of 4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

There total 1 articles about 4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 150-76-5
4-methoxy-phenol

: 191331-97-2
4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

Guidance literature:: 4-methoxy-phenol; With potassium hydroxide; In dimethyl sulfoxide; at 23 ℃; for 0.166667h;

2-(2-bromoethoxy)tetrahydropyran; In dimethyl sulfoxide; at 23 ℃; for 16h;
DOI:10.1016/j.bmc.2019.02.039

Reference yield: 100.0%

: 191331-97-2
4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

: 5394-57-0
2-(4-methoxyphenoxy)ethanol

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; at 23 ℃; for 16h;
DOI:10.1016/j.bmc.2019.02.039

Reference yield:

: 191331-97-2
4-methoxyphenoxyethyl tetrahydro-2H-pyran-2-yl ether

: 2-(4-methoxyphenoxy)ethyl ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridinium p-toluenesulfonate / methanol / 48 h / Ambient temperature

2: 64 percent / pyridine, 4-(dimethylamino)pyridine / 3 h / Ambient temperature

With pyridine; dmap; pyridinium p-toluenesulfonate; In methanol;
DOI:10.1021/jm9607616