[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

Base Information

Chemical Name:[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester
CAS No.:1075747-94-2
Molecular Formula:C₂₁H₂₅N₃O₄
Molecular Weight:383.447
Hs Code.:

Synonyms:[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

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Chemical Property of [3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

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Technology Process of [3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

There total 3 articles about [3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1075747-93-1
[3-(2-amino-4,5-dimethoxyphenylcarbamoyl)propyl]methylcarbamic acid benzyl ester

: 1075747-94-2
[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

Guidance literature:: [3-(2-amino-4,5-dimethoxyphenylcarbamoyl)propyl]methylcarbamic acid benzyl ester; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene; at 150 ℃; for 2h; Microwave irradiation;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 131076-14-7
4,5-dimethoxy-1,2-phenylenediamine hydrochloride salt

: 1075747-94-2
[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

2: toluene-4-sulfonic acid / N,N-dimethyl-formamide; toluene / 2 h / 150 °C / Microwave irradiation

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 98008-66-3
4-{[(benzyloxy)carbonyl](methyl)amino}butanoic acid

: 1075747-94-2
[3-(5,6-dimethoxy-1H-benzoimidazol-2-yl)propyl]methylcarbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

2: toluene-4-sulfonic acid / N,N-dimethyl-formamide; toluene / 2 h / 150 °C / Microwave irradiation

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;