N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide
• CAS No.: 460743-54-8
• Molecular Formula: C₃₃H₄₇N₃O₄S₂
• Molecular Weight: 613.886

Synonyms:N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide

Chemical Property of N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

benzylamine (100-46-9) + (S)-2-((R)-sec-butyl)-1-tosylaziridine (427892-72-6) → N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide (460743-54-8)

Guidance literature:

In methanol; for 72h; Heating;

DOI:10.1016/S0957-4166(02)00102-7

Reference yield: 95.0%

N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide (460743-54-8) → (2S,6S)-1,7-di-p-toluenesulfonyl-2,6-di(1-methylpropyl)-1,4,7-triazaheptane (497085-99-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; for 18h;

DOI:10.1039/b204818c

Reference yield: 67.0%

1,2-bis-tosyloxyethane (6315-52-2) + N-(1-{N'-[2-{4-methylbenzenesulfonylamino}-3-methyl-pentyl]aminomethyl}-2-methylbutyl)-4-methylbenzenesulfonamide (460743-54-8) → (S)-4-benzyl-2-(1-methylpropyl)-1-(4-methylbenzenesulfonyl)piperazine

Guidance literature:

With potassium carbonate; In acetonitrile; for 72h; Heating;

DOI:10.1039/b204818c

upstream raw materials:

benzylamine

(S)-2-((R)-sec-butyl)-1-tosylaziridine

Downstream raw materials:

(2S,6S)-1,7-di-p-toluenesulfonyl-2,6-di(1-methylpropyl)-1,4,7-triazaheptane

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