(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

Base Information

Chemical Name:(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester
CAS No.:134166-91-9
Molecular Formula:C₃₇H₄₂NO₆PS₂
Molecular Weight:691.849
Hs Code.:

Synonyms:(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

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Technology Process of (S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

There total 3 articles about (S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 134166-87-3
(S)-2-tert-Butoxycarbonylamino-3-hydroxy-propionic acid di-p-tolylmethyl ester

: Dithiophosphoric acid S,S'-di-o-tolyl ester; compound with cyclohexylamine

: 134166-91-9
(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

Guidance literature:: With pyridine; 1H-tetrazole; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride;
DOI:10.1016/S0040-4039(00)79664-X

Reference yield:

: 3262-72-4
(S)-N-(tert-butoxycarbonyl)serine

: 134166-91-9
(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 40percent peracetic acid, I₂ / CH₂Cl₂ / 0 °C

2: 75 percent / isodurenedisulfonyl chloride, 1H-tetrazole, pyridine

With pyridine; 1H-tetrazole; peracetic acid; iodine; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)79664-X

Reference yield:

: 55816-25-6
bis(4-methylphenyl)methanone hydrazone

: 134166-91-9
(S)-3-(Bis-o-tolylsulfanyl-phosphoryloxy)-2-tert-butoxycarbonylamino-propionic acid di-p-tolylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 40percent peracetic acid, I₂ / CH₂Cl₂ / 0 °C

2: 75 percent / isodurenedisulfonyl chloride, 1H-tetrazole, pyridine

With pyridine; 1H-tetrazole; peracetic acid; iodine; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)79664-X