lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

Base Information

Chemical Name:lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique
CAS No.:54815-41-7
Molecular Formula:C₁₅H₁₈O₂Se
Molecular Weight:309.267
Hs Code.:

Synonyms:lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

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Chemical Property of lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

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Technology Process of lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

There total 6 articles about lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 99957-07-0
acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

: 54815-41-7
lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

Guidance literature:: With phosphoric acid; at 110 ℃; for 6h;

Reference yield:

: 1552-91-6
cyclohexylideneacetic acid

: 54815-41-7
lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 1.) LDA / tetrahydrofuran / 1.) 45 deg C, 1 h, 2.) 40 deg C, 2 h

2: 50 percent / H₃PO₄ / 6 h / 110 °C

With phosphoric acid; lithium diisopropyl amide; In tetrahydrofuran;

Reference yield:

: 1552-92-7
ethyl cyclohexylideneacetate

: 54815-41-7
lactone de l'acide 3-phenylseleno-2-(cis-2'-hydroxycyclohexyl)-propanoique

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / 30percent aq. NaOH / ethanol / 3 h / Heating

2: 82 percent / 1.) LDA / tetrahydrofuran / 1.) 45 deg C, 1 h, 2.) 40 deg C, 2 h

3: 50 percent / H₃PO₄ / 6 h / 110 °C

With sodium hydroxide; phosphoric acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol;