acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

Base Information

Chemical Name:acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique
CAS No.:99957-07-0
Molecular Formula:C₁₅H₁₈O₂Se
Molecular Weight:309.267
Hs Code.:

Synonyms:acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

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Chemical Property of acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

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Technology Process of acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

There total 3 articles about acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 60466-50-4
α-bromo-α-(phenylseleno)methane

: 1552-91-6
cyclohexylideneacetic acid

: 99957-07-0
acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) 45 deg C, 1 h, 2.) 40 deg C, 2 h;

Reference yield:

: 1552-92-7
ethyl cyclohexylideneacetate

: 99957-07-0
acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 30percent aq. NaOH / ethanol / 3 h / Heating

2: 82 percent / 1.) LDA / tetrahydrofuran / 1.) 45 deg C, 1 h, 2.) 40 deg C, 2 h

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 99957-07-0
acide 3-phenylseleno-2-(1'-cyclohexenyl)-propanoique

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / benzoic acid / benzene / 48 h / Heating

2: 81 percent / 30percent aq. NaOH / ethanol / 3 h / Heating

3: 82 percent / 1.) LDA / tetrahydrofuran / 1.) 45 deg C, 1 h, 2.) 40 deg C, 2 h

With sodium hydroxide; benzoic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; benzene;