N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

Base Information

Chemical Name:N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine
CAS No.:136089-24-2
Molecular Formula:C₂₁H₃₆N₂O
Molecular Weight:332.53
Hs Code.:

Synonyms:N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

Chemical Property:

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Technology Process of N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

There total 9 articles about N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17380-62-0
1-phenylcyclopentanecarboxylic acid chloride

: 136089-24-2
N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃, pentane / CHCl₃; H₂O / 1 h / Ambient temperature

2: 74 percent / Red-Al / toluene / Heating

3: NaBH₃CN / acetonitrile; H₂O / 1 h / Ambient temperature

With sodium cyanoborohydride; sodium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; pentane; In chloroform; water; toluene; acetonitrile;
DOI:10.1021/jm00115a002

Reference yield:

: 136089-18-4
[2-(2-Azido-ethoxy)-ethyl]-diethyl-amine

: 136089-24-2
N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / ethanol / 48 h / 2068.6 Torr / Ambient temperature

2: NaHCO₃, pentane / CHCl₃; H₂O / 1 h / Ambient temperature

3: 74 percent / Red-Al / toluene / Heating

4: NaBH₃CN / acetonitrile; H₂O / 1 h / Ambient temperature

With hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; pentane; palladium on activated charcoal; In ethanol; chloroform; water; toluene; acetonitrile;
DOI:10.1021/jm00115a002

Reference yield:

: 140-82-9
2-[2-(diethylamino)ethoxy] ethanol

: 136089-24-2
N-<2-<2-(diethylamino)ethoxy>ethyl>-N-methyl-1-phenyl-1-cyclopentanemethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: zinc-azide-bispyridine complex, triphenylphosphine, diisopropyl azodicarboxylate / toluene / 2 h / Ambient temperature

2: H₂ / 10percent Pd/C / ethanol / 48 h / 2068.6 Torr / Ambient temperature

3: NaHCO₃, pentane / CHCl₃; H₂O / 1 h / Ambient temperature

4: 74 percent / Red-Al / toluene / Heating

5: NaBH₃CN / acetonitrile; H₂O / 1 h / Ambient temperature

With Zn(N₃)2/bis-pyridine complex; di-isopropyl azodicarboxylate; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; pentane; palladium on activated charcoal; In ethanol; chloroform; water; toluene; acetonitrile;
DOI:10.1021/jm00115a002