sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

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Chemical Name:sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate
CAS No.:130130-28-8
Molecular Formula:C₂₄H₂₈N₇O₈S*Na
Molecular Weight:597.584
Hs Code.:

Synonyms:sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

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Chemical Property of sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

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Technology Process of sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

There total 5 articles about sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 130130-33-5
benzyl 6β-<(2R)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>-2-<4-<(4-nitrobenzyl)oxycarbonylamino>phenyl>acetamido>-6α-formamidopenicillanate

: 130130-28-8
sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 74109-32-3
4-nitrobenzyl phenylcarbamate

: 130130-28-8
sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: 24 percent / conc. H₂SO₄ / acetic acid / 1 h

2: 32 percent / N,N'-dicyclohexylcarbodi-imide / ethyl acetate / 3 h / Ambient temperature

3: 94 percent / aq. NaHCO₃, H₂ / 10percent Pd/C / tetrahydrofuran / 2 h / Ambient temperature

With sulfuric acid; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; acetic acid; ethyl acetate;

Reference yield:

: 77579-89-6
D,L-2-[(4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino]-2-hydroxyacetic acid

: 130130-28-8
sodium 6β-<(2R)-2-(4-aminophenyl)-2-<4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-6α-formamidopenicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: 24 percent / conc. H₂SO₄ / acetic acid / 1 h

2: 32 percent / N,N'-dicyclohexylcarbodi-imide / ethyl acetate / 3 h / Ambient temperature

3: 94 percent / aq. NaHCO₃, H₂ / 10percent Pd/C / tetrahydrofuran / 2 h / Ambient temperature

With sulfuric acid; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; acetic acid; ethyl acetate;