DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

Base Information

Chemical Name:DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol
CAS No.:142573-32-8
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:

Synonyms:DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

Chemical Property:

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Technology Process of DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

There total 5 articles about DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 142573-32-8
DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid / acetonitrile / 0.25 h

2: 1.) NaH / 1.) N,N-DMF, 0 deg C, 30 min, 2.) 1 h

With sodium hydride; toluene-4-sulfonic acid; In acetonitrile;

Reference yield:

: 142573-30-6
(1R,2S,4R)-2-Hydroxymethyl-cyclohexane-1,4-diol

: 142573-32-8
DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid / acetonitrile / 0.25 h

2: 1.) NaH / 1.) N,N-DMF, 0 deg C, 30 min, 2.) 1 h

With sodium hydride; toluene-4-sulfonic acid; In acetonitrile;

Reference yield:

: 19800-01-2,38263-55-7,38263-56-8,64589-27-1
(+/-)-endo-7-oxabicyclo<2.2.1>-heptane-2-carboxylic acid

: 142573-32-8
DL-(1,5/4)-4,7-O-benzylidene-1-O-methyl-5-C-hydroxymethyl-1,4-cyclohexanediol

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / 85percent HOAc, H₂SO₄ / 20 h / 80 °C

2: BH₃ / tetrahydrofuran / 48 h / Ambient temperature

3: p-toluenesulfonic acid / acetonitrile / 0.25 h

4: 1.) NaH / 1.) N,N-DMF, 0 deg C, 30 min, 2.) 1 h

With sulfuric acid; borane; sodium hydride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; acetonitrile;