.beta.-D-Glucopyranose, 1-thio-, 2,3,4,6-tetraacetate 1-(dimethylcarbamodithioate)

Base Information

• Chemical Name: .beta.-D-Glucopyranose, 1-thio-, 2,3,4,6-tetraacetate 1-(dimethylcarbamodithioate)
• CAS No.: 19200-24-9
• Molecular Formula: C₁₇H₂₅NO₉S₂
• Molecular Weight: 451.519
• Mol file: 19200-24-9.mol

Synonyms:Glucopyranose,1-thio-, 2,3,4,6-tetraacetate 1-(dimethyldithiocarbamate), b-D- (8CI); Carbamic acid,dimethyldithio-, b-D-glucopyranosylester, 2,3,4,6-tetraacetate

Chemical Property of .beta.-D-Glucopyranose, 1-thio-, 2,3,4,6-tetraacetate 1-(dimethylcarbamodithioate)

Chemical Property:

• PSA: 175.06000
• LogP: 0.64920

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of .beta.-D-Glucopyranose, 1-thio-, 2,3,4,6-tetraacetate 1-(dimethylcarbamodithioate)

There total 2 articles about .beta.-D-Glucopyranose, 1-thio-, 2,3,4,6-tetraacetate 1-(dimethylcarbamodithioate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N,N-dimethyl β-D-glucopyranosyl dithiocarbamate (19200-26-1) + acetic anhydride (108-24-7) → 2,3,4,6-tetra-O-acetyl N,N-dimethyl S-β-glucopyranosyl dithiocarbamate (19200-24-9)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1039/d1ob00311a

Reference yield:

→ 2,3,4,6-tetra-O-acetyl N,N-dimethyl S-β-glucopyranosyl dithiocarbamate (19200-24-9)

Guidance literature:

2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl-bromid, Erw. mit Natrium-N,N-dimethyl-dithiocarbamat/Aceton;

upstream raw materials:

N,N-dimethyl β-D-glucopyranosyl dithiocarbamate

acetic anhydride

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