carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Base Information

Chemical Name:carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester
CAS No.:925461-72-9
Molecular Formula:C₁₈H₂₆O₄Si
Molecular Weight:334.488
Hs Code.:

Synonyms:carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Suppliers and Price of carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

There total 3 articles about carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 925462-31-3
carbonic acid allyl ester 2-oxo-2-phenyl-ethyl ester

: 69739-34-0
t-butyldimethylsiyl triflate

: 925461-72-9
carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.166667h;
DOI:10.1021/ja067342a

Reference yield:

: 582-24-1
1-phenyl-2-hydroxyethanone

: 925461-72-9
carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / CH₂Cl₂ / 0.5 h / -78 °C

2: 83 percent / Et₃N / CH₂Cl₂ / 0.17 h / -78 - 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1021/ja067342a

Reference yield:

: 70-11-1
α-bromoacetophenone

: 925461-72-9
carbonic acid allyl ester (Z)-2-(tert-butyl-dimethyl-silanoxy)-2-phenyl-vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / dimethylformamide / 20 °C

2: 83 percent / Et₃N / CH₂Cl₂ / 0.17 h / -78 - 20 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja067342a