ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

Base Information

Chemical Name:ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside
CAS No.:1431142-91-4
Molecular Formula:C₂₂H₃₄O₅SSi
Molecular Weight:438.66
Hs Code.:

Synonyms:ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

Chemical Property:

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Technology Process of ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

There total 1 articles about ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85272-31-7
di-tert-butylsilyl bis(trifluoromethanesulfonate)

: 118924-06-4
ethyl 1-thio-α-D-arabinofuranoside

: 1431142-91-4
ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane; N,N-dimethyl-formamide / 4 h / -5 °C

2: pyridine / 6 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc00042g

Reference yield: 87.0%

: 1431142-91-4
ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

: 1379681-45-4
ethyl 2-O-benzoyl-1-thio-α-D-arabinofuranoside

Guidance literature:: With pyridine; pyridine hydrofluoride; In tetrahydrofuran; at 0 - 20 ℃; for 5h;
DOI:10.1039/c3cc00042g

Reference yield:

: 1431142-91-4
ethyl 2-O-benzoyl-3,5-O-(di-tert-butylsilanediyl)-1-thio-α-D-arabinofuranoside

: 1431142-93-6
C₄₄H₃₈O₉S

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrofluoride; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; pyridine hydrofluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3cc00042g