C₃₅H₄₅NO₇

Base Information

Chemical Name:C₃₅H₄₅NO₇
CAS No.:1308271-91-1
Molecular Formula:C₃₅H₄₅NO₇
Molecular Weight:591.745
Hs Code.:

C<sub>35</sub>H<sub>45</sub>NO<sub>7</sub>

Synonyms:C₃₅H₄₅NO₇

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Chemical Property of C₃₅H₄₅NO₇

Chemical Property:

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Technology Process of C₃₅H₄₅NO₇

There total 17 articles about C₃₅H₄₅NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276112-41-4
C₃₅H₄₃NO₅

: 1308271-91-1
C₃₅H₄₅NO₇

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

: 1308271-84-2
C₂₇H₂₇NO₅

: 1308271-91-1
C₃₅H₄₅NO₇

Guidance literature:: Multi-step reaction with 12 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

3: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 2 h / 0 °C

5: tetrahydrofuran / 1.5 h / -78 °C

6: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

7: pyridine / 12 h / 0 - 20 °C

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; triethylamine / toluene / 0.5 h / Reflux

9: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

10: sodium periodate / tetrahydrofuran; water / 3.5 h / 0 - 20 °C

11: t-butyldimethylsiyl triflate / toluene / 9 h / -78 °C

12: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; t-butyldimethylsiyl triflate; ammonium formate; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

: 1308271-86-4
C₂₇H₂₉NO₅

: 1308271-91-1
C₃₅H₄₅NO₇

Guidance literature:: Multi-step reaction with 11 steps

1: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 2 h / 0 °C

4: tetrahydrofuran / 1.5 h / -78 °C

5: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

6: pyridine / 12 h / 0 - 20 °C

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; triethylamine / toluene / 0.5 h / Reflux

8: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

9: sodium periodate / tetrahydrofuran; water / 3.5 h / 0 - 20 °C

10: t-butyldimethylsiyl triflate / toluene / 9 h / -78 °C

11: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; t-butyldimethylsiyl triflate; ammonium formate; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.01.018