N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

Base Information

Chemical Name:N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester
CAS No.:1610355-13-9
Molecular Formula:C₃₃H₃₂NO₈P
Molecular Weight:601.593
Hs Code.:

Synonyms:N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

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Chemical Property of N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

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Technology Process of N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

There total 1 articles about N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 175291-56-2
Fmoc-L-Thr(HPO₃Bzl)-OH

: 100-51-6,185532-71-2
benzyl alcohol

: 1610355-13-9
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1002/cbdv.201300202

Reference yield: 60.0%

: 53064-79-2
iodomethyl pivaloate

: 1610355-13-9
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-threonine [phenylmethyl hydrogen Phosphate (ester)]phenylmethyl ester

: 1629149-57-0
benzyl O-[(benzyloxy){[(2,2-dimethylpropanoyl)oxy]methoxy}phosphoryl]-N-{[(9H-fluoren-9-yl)methoxy]carbonyl}-L-threoninate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/cbdv.201300202