C₁₅H₁₃ClN₂O₂

Base Information

Chemical Name:C₁₅H₁₃ClN₂O₂
CAS No.:1429500-87-7
Molecular Formula:C₁₅H₁₃ClN₂O₂
Molecular Weight:288.733
Hs Code.:

C<sub>15</sub>H<sub>13</sub>ClN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₅H₁₃ClN₂O₂

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Chemical Property of C₁₅H₁₃ClN₂O₂

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Technology Process of C₁₅H₁₃ClN₂O₂

There total 5 articles about C₁₅H₁₃ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429500-16-2
7-(3-chlorophenyl)-4-(2-hydroxyethyl)-3,4-dihydropyrrolo[1,2-a]pyrazin-1(2H)-one

: 1429500-87-7
C₁₅H₁₃ClN₂O₂

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; at 80 ℃; for 3h;

Reference yield:

: 1429500-38-8
ethyl [7-(3-chlorophenyl)-1-oxo-1,2,3,4-tetrahydropyrrolo[1,2-a]pyrazin-4-yl]acetate

: 1429500-87-7
C₁₅H₁₃ClN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h

2.2: 18 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C

With water; N-ethyl-N,N-diisopropylamine; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 63503-60-6
3-chlorophenylboronic acid

: 1429500-87-7
C₁₅H₁₃ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere

2.1: water; lithium hydroxide / tetrahydrofuran / 18 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h

3.2: 18 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; caesium carbonate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; water; ethyl acetate;