2,4-DIETHOXYBENZOIC ACID

Base Information

• Chemical Name: 2,4-DIETHOXYBENZOIC ACID
• CAS No.: 19074-30-7
• Molecular Formula: C11H14 O4
• Molecular Weight: 210.23
• Hs Code.: 2918990090
• Mol file: 19074-30-7.mol

Synonyms:2,4-Diethoxybenzoicacid

Chemical Property of 2,4-DIETHOXYBENZOIC ACID

Chemical Property:

• Vapor Pressure: 3.74E-05mmHg at 25°C
• Melting Point: 100-103 °C(lit.)
• Refractive Index: 1.521
• Boiling Point: 338.7°C at 760 mmHg
• PKA: 4.50±0.10(Predicted)
• Flash Point: 129.5°C
• PSA: 55.76000
• Density: 1.148g/cm³
• LogP: 2.18220

Purity/Quality:

98%Min ^*data from raw suppliers

2,4-Diethoxybenzoic acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-DIETHOXYBENZOIC ACID

There total 11 articles about 2,4-DIETHOXYBENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 2,4-diethoxybenzoate → 2,4-diethoxybenzoic acid (19074-30-7)

Guidance literature:

methyl 2,4-diethoxybenzoate; In water; Reflux;

With hydrogenchloride; In water;

DOI:10.1002/chem.201702742

Reference yield:

2,4-diethoxy-benzaldehyde (22924-16-9) → 2,4-diethoxybenzoic acid (19074-30-7)

Guidance literature:

With potassium permanganate; In acetone;

DOI:10.1016/0031-9422(74)80254-2

Reference yield:

diethyl sulfate (64-67-5) + 4-hydroxysalicylic acid (89-86-1) → 2,4-diethoxybenzoic acid (19074-30-7)

Guidance literature:

With sodium hydroxide;

DOI:10.1002/ardp.19582910905

upstream raw materials:

diethyl sulfate

4-hydroxysalicylic acid

2,4-diethoxy-benzoic acid ethyl ester

2,4-diethoxy-benzaldehyde

Downstream raw materials:

2′,4′-diethoxyacetophenone

5-acetoacetyl-2,4-diethoxy-benzoic acid ethyl ester

2,4-diethoxy-benzoic acid-(2-diethylamino-ethyl ester)

5-acetyl-2,4-diethoxy-benzoic acid ethyl ester

Refernces

• 1、 Satam, Manjaree A.,Raut, Rajesh K.,Tathe, Abhinav B.,Sekar. "Synthesis and characterization of molecules containing thiazole and oxazole moieties and study of ESIPT phenomenon". . p. 1237 - 1248. Retrieved 2013/01/15.