1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

Base Information

Chemical Name:1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)
CAS No.:1470259-83-6
Molecular Formula:C₄₅H₃₂F₁₂O₁₂
Molecular Weight:992.723
Hs Code.:

Synonyms:1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

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Chemical Property of 1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

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Technology Process of 1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

There total 1 articles about 1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 383-63-1
ethyl trifluoroacetate,

: 153088-89-2
C₃₇H₃₆O₈

: 1470259-83-6
1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

Guidance literature:: C₃₇H₃₆O₈; With sodium methylate; In tetrahydrofuran; at 20 ℃; for 0.166667h;

ethyl trifluoroacetate,; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c3tc31181c

Reference yield: 95.0%

: erbium(III) nitrate hexahydrate

: 1470259-83-6
1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

: 1643-19-2
tetrabutylammomium bromide

: C₄₅H₂₈F₁₂O₁₂^(4-)*Er⁽³⁺⁾*C₁₆H₃₆N⁽¹⁺⁾

Guidance literature:: erbium(III) nitrate hexahydrate; 1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione); With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 50 ℃; for 6h;

tetrabutylammomium bromide; In tetrahydrofuran; ethanol; water; at 50 ℃; for 6h;
DOI:10.1039/c3tc31181c

Reference yield: 95.0%

: ytterbium(III) nitrate hexahydrate

: 1470259-83-6
1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione)

: 1643-19-2
tetrabutylammomium bromide

: C₄₅H₂₈F₁₂O₁₂^(4-)*Yb⁽³⁺⁾*C₁₆H₃₆N⁽¹⁺⁾

Guidance literature:: ytterbium(III) nitrate hexahydrate; 1,1'-(4,4'-(2,2-bis((4-(4,4,4-trifluoro-3-oxobutanoyl)phenoxy)methyl)propane-1,3-diyl)bis(oxy)bis(4,1-phenylene))bis(4,4,4-trifluorobutane-1,3-dione); With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 50 ℃; for 6h;

tetrabutylammomium bromide; In tetrahydrofuran; ethanol; water; at 50 ℃; for 6h;
DOI:10.1039/c3tc31181c