methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside

Base Information

• Chemical Name: methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside
• CAS No.: 122805-35-0
• Molecular Formula: C₁₇H₂₁IO₆
• Molecular Weight: 448.255

Synonyms:methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside

Chemical Property of methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside

Chemical Property:

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Technology Process of methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside

There total 4 articles about methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 4-O-benzoyl-2,3-O-isopropylidene-6-O-tosyl-α-D-mannopyranoside (122805-34-9) → methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside (122805-35-0)

Guidance literature:

With sodium iodide; In acetonitrile; for 5h; Yield given; Heating;

DOI:10.1016/0008-6215(89)85108-0

Reference yield:

benzoyl chloride (98-88-4) → methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside (122805-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: sodium iodide / acetonitrile / 5 h / Heating

With pyridine; sodium iodide; In acetonitrile;

DOI:10.1016/0008-6215(89)85108-0

Reference yield:

methyl 2,3-O-isopropylidene-6-O-p-toluenesulfonyl-α-D-mannopyranoside (112612-45-0) → methyl 4-O-benzoyl-6-deoxy-6-iodo-2,3-isopropylidene-α-D-mannopyranoside (122805-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: sodium iodide / acetonitrile / 5 h / Heating

With pyridine; sodium iodide; In acetonitrile;

DOI:10.1016/0008-6215(89)85108-0

upstream raw materials:

methyl 4-O-benzoyl-2,3-O-isopropylidene-6-O-tosyl-α-D-mannopyranoside

benzoyl chloride

methyl 2,3-O-isopropylidene-6-O-p-toluenesulfonyl-α-D-mannopyranoside

methyl 2,3-O-isopropylidene-α-D-mannopyranoside

Downstream raw materials:

methyl 4-O-benzoyl-α-D-rhamnopyranoside

methyl 2,4-di-O-benzoyl-α-D-rhamnopyranoside

Benzoic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-bromo-2-methyl-tetrahydro-pyran-3-yl ester

methyl 3,4-di-O-benzoyl-α-D-rhamnopyranoside

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