C₂₉H₄₄NO₁₀P

Base Information

• Chemical Name: C₂₉H₄₄NO₁₀P
• CAS No.: 1160508-95-1
• Molecular Formula: C₂₉H₄₄NO₁₀P
• Molecular Weight: 597.643
• Mol file: 1160508-95-1.mol

Synonyms:C₂₉H₄₄NO₁₀P

Chemical Property of C₂₉H₄₄NO₁₀P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₉H₄₄NO₁₀P

There total 1 articles about C₂₉H₄₄NO₁₀P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Diethyl methylphosphonate (683-08-9) + Boc-L-phenylalaninal (72155-45-4) + ethyl phosphodichloridite (1498-51-7) + 1,2:3,4-di-O-isopropylidene-α-D-galactopyranose (4064-06-6) → C29H44NO10P (1160508-95-1)

Guidance literature:

Diethyl methylphosphonate; ethyl phosphodichloridite; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 3h;

1,2:3,4-di-O-isopropylidene-α-D-galactopyranose; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h;

Boc-L-phenylalaninal; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 20 ℃; for 12h; Further stages.;

DOI:10.1002/hc.20450

Reference yield: 93.0%

C29H44NO10P (1160508-95-1) → C29H46NO10P (1160509-02-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 12h; under 22502.3 Torr;

DOI:10.1002/hc.20450

upstream raw materials:

Diethyl methylphosphonate

Boc-L-phenylalaninal

ethyl phosphodichloridite

1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Downstream raw materials:

C₂₉H₄₆NO₁₀P