methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

Base Information

Chemical Name:methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate
CAS No.:137841-64-6
Molecular Formula:C₁₉H₃₀N₂O₂S₂
Molecular Weight:382.591
Hs Code.:

Synonyms:methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

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Chemical Property of methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

Chemical Property:

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Technology Process of methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

There total 2 articles about methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 32687-77-7
3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanoic acid hydrazide

: 74-88-4
methyl iodide

: 137841-64-6
methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

Guidance literature:: carbon disulfide; 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanoic acid hydrazide; With potassium hydroxide; In ethanol; at 0 - 20 ℃; for 28h;

methyl iodide; In ethanol; at 20 ℃; for 6h;
DOI:10.1080/00304948.2020.1823768

Reference yield:

: 6386-38-5
methyl 3-(4-hydroxy-3,5-di-tert-butyl)phenylpropanoate

: 137841-64-6
methyl 2-(3-(4-hydroxy-3,5-di-tert-butylphenyl)propanoyl)hydrazine-1-carbothionate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / hydrazine monohydrate / methanol / 2 h / Heating

2: 1.) CH₃OH, a) 0 deg C, 2 h, b) RT, 4 h, 2.) CH₃OH, overnight

With hydrazine hydrate; In methanol;
DOI:10.1002/jhet.5570310625