Technology Process of C17H15F4N5O
There total 5 articles about C17H15F4N5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
for 16h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -78 °C
1.2: -78 - 20 °C
2.1: diethyl ether / -5 - 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
4.1: hydrazine hydrate / ethanol / 16 h / Reflux
With
n-butyllithium; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; diethyl ether; ethanol; hexane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper / dimethyl sulfoxide / 1 h / 20 °C
1.2: 15 h / 20 °C
2.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -78 °C
2.2: -78 - 20 °C
3.1: diethyl ether / -5 - 20 °C
4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
4.2: 0 - 20 °C / Inert atmosphere
5.1: hydrazine hydrate / ethanol / 16 h / Reflux
With
n-butyllithium; copper; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; diethyl ether; ethanol; hexane; dimethyl sulfoxide;