Technology Process of C26H24N4O2
There total 4 articles about C26H24N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
L-alanine methyl ester hydrochloride;
With
sodium carbonate;
In
N,N-dimethyl-formamide;
at 201 ℃;
for 1h;
Inert atmosphere;
4'-(4-bromomethylphenyl)-2,2':6',2''-terpyridine;
In
N,N-dimethyl-formamide;
at 20 - 45 ℃;
for 18h;
Inert atmosphere;
DOI:10.1002/ejic.201200100
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonia; potassium hydroxide / ethanol; water / 36 h / Reflux
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux; Inert atmosphere
3.1: sodium carbonate / N,N-dimethyl-formamide / 1 h / 201 °C / Inert atmosphere
3.2: 18 h / 20 - 45 °C / Inert atmosphere
With
N-Bromosuccinimide; ammonia; sodium carbonate; potassium hydroxide; dibenzoyl peroxide;
In
tetrachloromethane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201200100
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonia; potassium hydroxide / ethanol; water / 36 h / Reflux
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / Reflux; Inert atmosphere
3.1: sodium carbonate / N,N-dimethyl-formamide / 1 h / 201 °C / Inert atmosphere
3.2: 18 h / 20 - 45 °C / Inert atmosphere
With
N-Bromosuccinimide; ammonia; sodium carbonate; potassium hydroxide; dibenzoyl peroxide;
In
tetrachloromethane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201200100