C₆H₄SH(S-SnBu₃)

Base Information

Chemical Name:C₆H₄SH(S-SnBu₃)
CAS No.:1192690-75-7
Molecular Formula:C₁₈H₃₂S₂Sn
Molecular Weight:431.294
Hs Code.:

C<sub>6</sub>H<sub>4</sub>SH(S-SnBu<sub>3</sub>)

Synonyms:C₆H₄SH(S-SnBu₃)

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Chemical Property of C₆H₄SH(S-SnBu₃)

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Technology Process of C₆H₄SH(S-SnBu₃)

There total 1 articles about C₆H₄SH(S-SnBu₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: polyborazylene

: 688-73-3
tri-n-butyl-tin hydride

: 1002-53-5
dibutylstannane

: 17534-15-5
Benzene-1,2-dithiol

: 10043-11-5
borane-ammonia complex

: (n-Bu)2Sn(1,2-benzenedithiolate)

: 1192690-75-7
C₆H₄SH(S-SnBu₃)

Guidance literature:: In tetrahydrofuran; byproducts: H2; C6H4(SH)2 (1.83 mmol) added to soln. of polyborazylene (0.61 mmol), mixt. heated overnight at 60°C, excess Bu3SnH (0.9 mmol) added (reacted for 12 h), soln. heated to 60°C, then nBu2SnH2 (4.86 mmol) added in four portions over 40 min; washing (toluene); deted. by (119)Sn NMR;
DOI:10.1002/anie.200900680

Reference yield: 83.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1192690-75-7
C₆H₄SH(S-SnBu₃)

: 1461-22-9
tributyltin chloride

Guidance literature:: In diethyl ether; byproducts: ortho-benzenedithiol; C6H4SH(S-SnBu3) reacted with HCl-Et2O; solid washed with Et2O and dried;
DOI:10.1039/b919383a