((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane
CAS No.:1190239-60-1
Molecular Formula:C₃₈H₅₉N₃O₃Si₂
Molecular Weight:662.076
Hs Code.:

((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

Synonyms:((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

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Chemical Property of ((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

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Technology Process of ((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

There total 2 articles about ((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1190239-54-3
((2R,3S,5S,6S)-3-(tert-butyldimethylsilyloxy)-6-((3E,5E)-7-(tert-butyldiphenylsilyloxy)-4,5-dimethylhepta-3,5-dienyl)-5-methyl-tetrahydro-2H-pyran-2-yl)methanol

: 1190239-60-1
((2E,4E)-7-((2S,3S,5S,6R)-6-(azidomethyl)-5-(tert-butyldimethylsilyloxy)-3-methyl-tetrahydro-2H-pyran-2-yl)-3,4-dimethylhepta-2,4-dienyloxy)(tert-butyl)diphenylsilane

Guidance literature:: ((2R,3S,5S,6S)-3-(tert-butyldimethylsilyloxy)-6-((3E,5E)-7-(tert-butyldiphenylsilyloxy)-4,5-dimethylhepta-3,5-dienyl)-5-methyl-tetrahydro-2H-pyran-2-yl)methanol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

With diphenyl phosphoryl azide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol901801h