Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Base Information

Chemical Name:Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride
CAS No.:128684-19-5
Molecular Formula:C₃₆H₅₀N₆O₆*ClH
Molecular Weight:699.291
Hs Code.:

Lys(CO(CH<sub>2</sub>)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Synonyms:Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Chemical Property:

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Technology Process of Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

There total 4 articles about Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13033-84-6
D-phenylalanine methyl ester hydrochloride

: 128684-19-5
Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / triethylamine / dimethylformamide / 16 h / Ambient temperature

2: 73 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), triethylamine / dimethylformamide

3: 4N aq. NaOH / methanol

4: 3N HCl, AcOH

With hydrogenchloride; sodium hydroxide; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00171a034

Reference yield:

: 128684-32-2
N-glutaryl-D-phenylalanine methyl ester

: 128684-19-5
Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / dicyclohexylcarbodiimide (DCCI), 1-hydroxybenzotriazole (HOBt), triethylamine / dimethylformamide

2: 4N aq. NaOH / methanol

3: 3N HCl, AcOH

With hydrogenchloride; sodium hydroxide; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00171a034

Reference yield:

: 128684-40-2
Boc-Lys(CO(CH₂)3CO-D-Phe-OMe)-D-Trp-(S)-(-)-2-methylbutylamide

: 128684-19-5
Lys(CO(CH₂)3CO-D-Phe-OH)-D-Trp-(S)-(-)-2-methylbutylamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 4N aq. NaOH / methanol

2: 3N HCl, AcOH

With hydrogenchloride; sodium hydroxide; acetic acid; In methanol;
DOI:10.1021/jm00171a034