Technology Process of C34H32FN3O5
There total 10 articles about C34H32FN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ml2000438
- Guidance literature:
-
C34H34FN3O5;
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 16h;
With
ammonium chloride;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: water; sodium hydroxide / methanol / 16 h / 20 °C / Inert atmosphere
2.1: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / -10 - 20 °C / Inert atmosphere
3.1: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran / 0.5 h / Inert atmosphere
4.2: 4 h / 20 °C / Inert atmosphere
5.1: TurboGrignard / tetrahydrofuran / 0.5 h / Inert atmosphere
5.2: 16 h / 20 °C / Inert atmosphere
6.1: Dess-Martin periodane / dichloromethane / 16 h / 20 °C / Inert atmosphere
With
pyridine; sodium tetrahydroborate; TurboGrignard; trifluoro-[1,3,5]triazine; water; sodium hydride; Dess-Martin periodane; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
6.1: Dess-Martin oxidation;
DOI:10.1021/ml2000438