Technology Process of C33H34N8
There total 16 articles about C33H34N8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 8h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 4.5 h / 0 - 20 °C
2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water / 2 h / 90 °C / Inert atmosphere
4: hydrogenchloride / ethyl acetate / 8 h / 20 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonium acetate / toluene / 120 °C
2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere
4: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water / 2 h / 90 °C / Inert atmosphere
5: hydrogenchloride / ethyl acetate / 8 h / 20 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ammonium acetate; potassium acetate; potassium carbonate;
In
1,2-dimethoxyethane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene;