N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

Base Information

Chemical Name:N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide
CAS No.:1321622-47-2
Molecular Formula:C₃₇H₅₇N₅O₆
Molecular Weight:667.889
Hs Code.:

Synonyms:N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

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Chemical Property of N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

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Technology Process of N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

There total 7 articles about N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.8%

: 1321622-65-4
N-(3-amino-2,2-dimethylpropyl)benzamide

: 1227379-44-3
C₂₅H₃₉N₃O₅

: 1321622-47-2
N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

Guidance literature:: With 2-hydroxypyridin; triethylamine; at 65 ℃;
DOI:10.1016/j.bmc.2011.05.059

Reference yield:

: 1321622-81-4
N-(3-azido-2,2-dimethylpropyl)benzamide

: 1321622-47-2
N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 25 °C

2: 2-hydroxypyridin; triethylamine / 65 °C

With 2-hydroxypyridin; palladium 10% on activated carbon; hydrogen; triethylamine; In methanol;
DOI:10.1016/j.bmc.2011.05.059

Reference yield:

: 111992-61-1
2-(3-bromo-2, 2-dimethylpropyl)-2,3-dihydro-1H-isoindole-1,3-dione

: 1321622-47-2
N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / N,N-dimethyl-formamide / 8 h / 100 °C

2: hydrazine hydrate / ethanol / 4 h / 80 °C

3: triethylamine / dichloromethane / 0 - 25 °C

4: palladium 10% on activated carbon; hydrogen / methanol / 25 °C

5: 2-hydroxypyridin; triethylamine / 65 °C

With 2-hydroxypyridin; sodium azide; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; triethylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.059