<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

Base Information

Chemical Name:<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide
CAS No.:175979-80-3
Molecular Formula:C₂₃H₃₁NO₃
Molecular Weight:369.504
Hs Code.:

Synonyms:<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

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Chemical Property of <1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

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Technology Process of <1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

There total 1 articles about <1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-30-5
2-methyl-1,2-epoxypropane

: 14980-86-0,42407-58-9
N-((1S,2S)-1-hydroxy-1-phenylpropan-2-yl)-N-methyl-3-phenylpropanamide

: 175979-80-3
<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

Guidance literature:: With lithium chloride; lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 -> 23 deg C, 2.) THF, 0 deg C, 4 h;
DOI:10.1021/jo952032o

Reference yield: 94.0%

: 175979-80-3
<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

: 175979-81-4
(S)-3-Benzyl-5,5-dimethyl-dihydro-furan-2-one

Guidance literature:: With sulfuric acid; In 1,4-dioxane; water; at 95 ℃; for 2h;
DOI:10.1021/jo952032o

Reference yield:

: 175979-80-3
<1S(2S),2S>-N-(2-hydroxy-1-methyl-2-phenylethyl)-4-hydroxy-N,4-dimethyl-2-(phenylmethyl)pentanamide

: (S)-2-Benzyl-4-methyl-pentane-1,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / sulfuric acid / H₂O; dioxane / 2 h / 95 °C

2: lithium aluminum hydride / diethyl ether / 0 °C

With lithium aluminium tetrahydride; sulfuric acid; In 1,4-dioxane; diethyl ether; water;
DOI:10.1021/jo952032o