4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

Base Information

Chemical Name:4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide
CAS No.:74671-33-3
Molecular Formula:C₂₄H₂₁N₃O₃
Molecular Weight:399.449
Hs Code.:

Synonyms:4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

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Chemical Property of 4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

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Technology Process of 4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

There total 1 articles about 4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 10314-06-4
4-phthalimidobutyryl chloride

: 530-50-7
1,1-Diphenylhydrazine

: 74671-33-3
4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

Guidance literature:: With triethylamine; In benzene; for 2h;
DOI:10.1007/BF00552776

Reference yield: 81.0%

: 74671-33-3
4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

: 74671-41-3
2-[2-(2-Amino-1-phenyl-1H-indol-3-yl)-ethyl]-isoindole-1,3-dione; hydrochloride

Guidance literature:: With trichlorophosphate; In dichloromethane; at 40 ℃; for 42h;
DOI:10.1007/BF00552776

Reference yield:

: 74671-33-3
4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-butyric acid N',N'-diphenyl-hydrazide

: 74671-47-9
2-Benzoylamino-1-phenyl-3-(2-phthalimidoethyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / POCl₃ / CH₂Cl₂ / 42 h / 40 °C

2: 80 percent / 2N NaOH / H₂O / 1 h

With sodium hydroxide; trichlorophosphate; In dichloromethane; water;
DOI:10.1007/BF00552776