1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Base Information

Chemical Name:1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine
CAS No.:256664-81-0
Molecular Formula:C₂₀H₂₆N₂O₂
Molecular Weight:326.439
Hs Code.:

Synonyms:1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Suppliers and Price of 1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

There total 2 articles about 1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100-52-7
benzaldehyde

: 103449-03-2
para-(tert-butyl)benzoic acid N',N'-dimethylhydrazine

: 256664-81-0
1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Guidance literature:: para-(tert-butyl)benzoic acid N',N'-dimethylhydrazine; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at 0 - 10 ℃; for 0.1h;

benzaldehyde; In tetrahydrofuran; cyclohexane;
DOI:10.1016/S0040-4039(99)01876-6

Reference yield:

: 1710-98-1
p-tert-butyl benzoyl chloride

: 256664-81-0
1-[2-(1-hydroxy-1-phenylmethyl)-4-(1,1-dimethylethyl)benzoyl]-2,2-dimethylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: CH₂Cl₂ / 10 °C

2.1: s-BuLi / tetrahydrofuran; cyclohexane / 0.1 h / 0 - 10 °C

2.2: 83 percent / tetrahydrofuran; cyclohexane

With sec.-butyllithium; In tetrahydrofuran; dichloromethane; cyclohexane; 1.1: Acylation / 2.1: metalation / 2.2: Substitution;
DOI:10.1016/S0040-4039(99)01876-6