(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

Base Information

Chemical Name:(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide
CAS No.:919529-11-6
Molecular Formula:C₄₀H₄₄N₄O₆S
Molecular Weight:708.879
Hs Code.:

(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

Synonyms:(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

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Chemical Property of (2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

Chemical Property:

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Technology Process of (2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

There total 1 articles about (2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-amino-3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]-methyl}phenyl)propanamide trifluoroacetic acid salt

: 102830-49-9
N-tert-butyloxycarbonyl-(S)-benzyl-N-(tert-butyloxycarbonyl)-D-cysteine

: 919529-11-6
(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

Guidance literature:: N-tert-butyloxycarbonyl-(S)-benzyl-N-(tert-butyloxycarbonyl)-D-cysteine; With HBTU; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

N-amino-3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]-methyl}phenyl)propanamide trifluoroacetic acid salt; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 18h; pH=10;

Reference yield: 39.6%

: 23911-25-3
ethylenediaminetetraacetic dianhydride

: 919529-11-6
(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

: 919529-21-8
2-{{[N-({4-[2-(N-{(2S)-2-[(tert-butoxy)carbonylamino]-3-(phenylmethylthio)propanoylamino}carbamoyl)ethyl]phenyl}methyl)carbamoyl]methyl}[2-({[N-({4-[2-(N-{(2S)-2-[(tert-butoxy)carbonylamino]-3-(phenylmethylthio)-propanoylamino}carbamoyl)ethyl]phenyl}methyl)carbamoyl]methyl}(carboxymethyl)amino)ethyl]amino}acetic acid

Guidance literature:: (2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide; With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

ethylenediaminetetraacetic dianhydride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 919529-11-6
(2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide

: 174267-71-1
3,9-Bis(tert-butoxycarbonylmethyl)-6-carboxymethyl-3,6,9-triazaundecanedioic acid-di-tert-butyl ester

: C₅₅H₈₇N₇O₁₃S

Guidance literature:: (2S)-2-[(tert-butoxy)carbonylamino]-N-[3-(4-{[(fluoren-9-ylmethoxy)carbonylamino]methyl}phenyl)propanoylamino]-3-(phenylmethylthio)-propanamide; With diethylamine; In acetonitrile; at 20 ℃; for 0.5h;

3,9-Bis(tert-butoxycarbonylmethyl)-6-carboxymethyl-3,6,9-triazaundecanedioic acid-di-tert-butyl ester; With HBTU; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;