4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

Base Information

Chemical Name:4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester
CAS No.:1350375-37-9
Molecular Formula:C₂₇H₃₆O₄Si
Molecular Weight:452.666
Hs Code.:

Synonyms:4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

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Chemical Property of 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

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Technology Process of 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

There total 4 articles about 4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1350375-38-0
1-allyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclohexanecarboxylic acid ethyl ester

: 1350375-37-9
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

Guidance literature:: With sodium periodate; osmium(VIII) oxide; In water; isopropyl alcohol; at 20 ℃; for 16h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1350375-37-9
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / 1,2-dichloro-ethane / 20 °C

2.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -77 °C

2.2: 1.33 h / -78 - 20 °C

3.1: osmium(VIII) oxide; sodium periodate / isopropyl alcohol; water / 16 h / 20 °C

With 1H-imidazole; sodium periodate; osmium(VIII) oxide; n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; water; 1,2-dichloro-ethane; isopropyl alcohol;

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 1350375-37-9
4-(tert-butyl-diphenyl-silanyloxy)-1-(2-oxo-ethyl)-cyclohexanecarboxylic acidmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / 1,2-dichloro-ethane / 20 °C

2.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -77 °C

2.2: 1.33 h / -78 - 20 °C

3.1: osmium(VIII) oxide; sodium periodate / isopropyl alcohol; water / 16 h / 20 °C

With 1H-imidazole; sodium periodate; osmium(VIII) oxide; n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; water; 1,2-dichloro-ethane; isopropyl alcohol;