1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

Base Information

Chemical Name:1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine
CAS No.:399560-02-2
Molecular Formula:C₁₇H₁₉N₇O₆S
Molecular Weight:449.447
Hs Code.:

Synonyms:1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

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Technology Process of 1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

There total 2 articles about 1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 399559-99-0
1-[(4-ethoxycarbonyl-3-methylthio-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroiminoimidazolidine

: 399560-02-2
1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

Guidance literature:: With dihydrogen peroxide; acetic acid; at 45 - 47 ℃; for 30h;
DOI:10.1002/jhet.5570380504

Reference yield:

: [(4-ethoxycarbonyl-3-methio-1-phenyl)pyrazol-5-yl]iminomethyl ethyl ether

: 399560-02-2
1-[(4-ethoxycarbonyl-3-methylsulfonyl-1-phenyl)pyrazol-5-yl]iminomethyl-2-nitroimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / sodium hydride / acetonitrile / 3 h / 20 °C

2: 67 percent / 30 percent aq. hydrogenperoxide; acetic acid / 30 h / 45 - 47 °C

With dihydrogen peroxide; sodium hydride; acetic acid; In acetonitrile;
DOI:10.1002/jhet.5570380504