(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

Base Information

Chemical Name:(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide
CAS No.:1322564-75-9
Molecular Formula:C₁₅H₁₅F₂N₅O₃
Molecular Weight:351.313
Hs Code.:

Synonyms:(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

Chemical Property:

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Technology Process of (S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

There total 2 articles about (S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 1322564-49-7
C₉H₈F₃N₃O₃

: 1322564-75-9
(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 80 ℃; for 1h; under 5171.62 Torr; Microwave irradiation;
DOI:10.1002/cjoc.201190200

Reference yield:

: 16583-08-7
2,3,4,5-tetrafluoro-6-nitrobenzoic acid

: 1322564-75-9
(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 24 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 80 °C / 5171.62 Torr / Microwave irradiation

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/cjoc.201190200

Reference yield:

: 1322564-75-9
(S)-2-(2,6-difluoro-4-nitro-3-(pyridin-2-ylmethylamino)phenylamino)propanamide

: C₁₅H₁₇F₂N₅O

Guidance literature:: With palladium 10% on activated carbon; ammonium formate; In tetrahydrofuran; ethanol; at 20 ℃;
DOI:10.1002/cjoc.201190200