iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

Base Information

Chemical Name:iron(II) nitrosyl meso-(tetraphenyl) porphyrinate
CAS No.:70622-46-7
Molecular Formula:C₄₄H₂₈FeN₅O
Molecular Weight:698.586
Hs Code.:

Synonyms:iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

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Chemical Property of iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

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Technology Process of iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

There total 5 articles about iron(II) nitrosyl meso-(tetraphenyl) porphyrinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16456-81-8,170645-84-8
meso-tetraphenylporphyrin iron(III) chloride

: sodium trioxodinitrate

: 70622-46-7
iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

Guidance literature:: In methanol; dichloromethane; (Ar); dropwise addn. of soln. of sodium trioxodinitrate in deareated MeOH to srirred soln. of FeTPPCl in min. volume of CH2Cl2 at room temp.; pptn. for 10 min, sepn. by centrifugation, dissolving in CH2Cl2, washingwith water, concn. of org. layer in vac., recrystn. from CH2Cl2/CH3OH;

Reference yield:

: 16456-81-8,170645-84-8
meso-tetraphenylporphyrin iron(III) chloride

: 1593-60-8
p-toluenesulfonylhydroxylamine

: 70622-46-7
iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

Guidance literature:: In methanol; dichloromethane; (Ar); dropwise addn. of soln. of toluenesulfohydroxamic acid in deareated MeOH to srirred soln. of FeTPPCl in min. volume of CH2Cl2 at room temp.; pptn. for 24 h, sepn. by centrifugation, dissolving in CH2Cl2, washing with water, concn. of org. layer in vac., recrystn. from CH2Cl2/CH3OH;

Reference yield:

: 42034-08-2
nitrosylcobalt(II) meso-tetraphenylporphyrinate

: 57715-43-2
[iron(III)(5,10,15,20-tetraphenyl-21H,23H-porphine)] perchlorate

: 125138-88-7
{(tetraphenylporphyrin)FeClO₄}⁽¹⁺⁾

: {(TPP)Co(NO)}⁽¹⁺⁾

: 70622-46-7
iron(II) nitrosyl meso-(tetraphenyl) porphyrinate

Guidance literature:: With N((CH₂)3CH₃)4ClO₄; In dichloromethane; Electrochem. Process; electrooxidn. in a thin layer cell (SCE electrode, electrolyte 0.1 M TBAP) by 1.1 V; not isolated, detd. by IR;