N'-benzyl-N',4-dimethylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-benzyl-N',4-dimethylbenzenesulfonohydrazide
• CAS No.: 1376001-73-8
• Molecular Formula: C₁₅H₁₈N₂O₂S
• Molecular Weight: 290.386
• Mol file: 1376001-73-8.mol

Synonyms:N'-benzyl-N',4-dimethylbenzenesulfonohydrazide

Chemical Property of N'-benzyl-N',4-dimethylbenzenesulfonohydrazide

Chemical Property:

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Technology Process of N'-benzyl-N',4-dimethylbenzenesulfonohydrazide

There total 1 articles about N'-benzyl-N',4-dimethylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-tolyl iodide (624-31-7) + 1-benzyl-1-methylhydrazine (3931-52-0) → N'-benzyl-N',4-dimethylbenzenesulfonohydrazide (1376001-73-8)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate; In 1,4-dioxane; at 70 ℃; for 16h; Inert atmosphere;

DOI:10.1039/c2ob07034k

upstream raw materials:

4-tolyl iodide

1-benzyl-1-methylhydrazine