N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Base Information

Chemical Name:N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide
CAS No.:887268-76-0
Molecular Formula:C₂₉H₂₅N₃O₅S
Molecular Weight:527.601
Hs Code.:

Synonyms:N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

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Chemical Property of N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

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Technology Process of N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

There total 1 articles about N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 99-57-0
2-hydroxy-5-nitroaniline

: 91425-33-1
N-hydroxysuccinimidyl 2-[(triphenylmethylthio)methylcarbonylamino]ethanoate

: 887268-76-0
N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: With dmap; In acetonitrile; at 60 ℃; for 4h;
DOI:10.1002/ejoc.200500810

Reference yield: 78.0%

: 887268-76-0
N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

: 887268-77-1
N-(5-amino-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: With hydrazine hydrate; nickel; In ethanol; 1,2-dichloro-ethane; for 2h;
DOI:10.1002/ejoc.200500810

Reference yield:

: 887268-76-0
N-(2-hydroxy-5-nitrophenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

: 887268-80-6
N-(4-isothiocyanato-2-hydroxyphenyl)-2-[(triphenylmethylthio)methylcarbonylamino]ethanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / hydrazine monohydrate / Raney nickel / 1,2-dichloro-ethane; ethanol / 2 h

2: 87 percent / tetrahydrofuran / 1 h / 20 °C

With hydrazine hydrate; nickel; In tetrahydrofuran; ethanol; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.200500810