2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE

Base Information

• Chemical Name: 2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE
• CAS No.: 18583-54-5
• Molecular Formula: C25H20 Cl2 P . Cl
• Molecular Weight: 457.767
• Hs Code.: 2931900090
• Mol file: 18583-54-5.mol

Synonyms:(2,6-Dichlorobenzyl)triphenylphosphoniumchloride (6CI); Phosphonium, (2,6-dichlorobenzyl)triphenyl-, chloride (8CI);Phosphonium, [(2,6-dichlorophenyl)methyl]triphenyl-, chloride (9CI)

Chemical Property of 2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE

Chemical Property:

• Melting Point: 117-119?°C(lit.)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 13.59000
• Density: g/cm³
• LogP: 3.49150

Purity/Quality:

98%min ^*data from raw suppliers

2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE

There total 2 articles about 2,6-DICHLOROBENZYL TRIPHENYLPHOSPHONIUM CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,3-Dichloro-2-chloromethyl-benzene (2014-83-7) + triphenylphosphine (603-35-0) → (2,6-dichlorobenzyl)triphenylphosphonium chloride (18583-54-5)

Guidance literature:

In benzene; for 1h; Heating;

DOI:10.1016/0040-4020(84)85121-2

Reference yield:

→ (2,6-dichlorobenzyl)triphenylphosphonium chloride (18583-54-5)

Guidance literature:

Reference yield: 83.0%

(2,6-dichlorobenzyl)triphenylphosphonium chloride (18583-54-5) + (E)-3-(2,6-dichlorophenyl)acrylaldehyde (99668-08-3) → C16H10Cl4 (89970-57-0) + C16H10Cl4 (89970-57-0) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; for 0.666667h;

DOI:10.1016/0040-4020(84)85121-2

upstream raw materials:

1,3-Dichloro-2-chloromethyl-benzene

triphenylphosphine

Downstream raw materials:

1-(2,6-Dichlorphenyl)-4-(m-nitrophenyl)-1,3-butadien

C₁₆H₁₀Cl₄

C₁₆H₁₀Cl₄

Triphenylphosphine oxide