C₆₄H₇₉N₅O₁₂P₂

Base Information

Chemical Name:C₆₄H₇₉N₅O₁₂P₂
CAS No.:1417729-48-6
Molecular Formula:C₆₄H₇₉N₅O₁₂P₂
Molecular Weight:1172.31
Hs Code.:

C<sub>64</sub>H<sub>79</sub>N<sub>5</sub>O<sub>12</sub>P<sub>2</sub>

Synonyms:C₆₄H₇₉N₅O₁₂P₂

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Chemical Property of C₆₄H₇₉N₅O₁₂P₂

Chemical Property:

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Technology Process of C₆₄H₇₉N₅O₁₂P₂

There total 17 articles about C₆₄H₇₉N₅O₁₂P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417729-46-4
C₆₉H₈₇N₅O₁₄P₂

: 1417729-48-6
C₆₄H₇₉N₅O₁₂P₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2cc35247h DOI:10.1002/chem.201301273

Reference yield:

: 5315-25-3
2-bromo-6-methylpyridine

: 1417729-48-6
C₆₄H₇₉N₅O₁₂P₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 65 °C / Inert atmosphere

2.1: nitric acid; sulfuric acid / 16 h / 0 - 100 °C

3.1: phosphorus tribromide / chloroform / 16 h / 60 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / toluene / 16 h / 125 °C / Inert atmosphere

5.1: Acetyl bromide / 16 h / 70 °C / Inert atmosphere

5.2: 0 °C

6.1: 72 h / 140 °C / Inert atmosphere

7.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / 65 °C / Inert atmosphere

8.1: 3 h / 120 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; copper(l) iodide; tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

10.1: ethanol; sodium / 50 °C / Inert atmosphere

11.1: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

12.1: potassium carbonate / acetonitrile / 1 h / 50 °C / Inert atmosphere

13.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Acetyl bromide; ethanol; sulfuric acid; tetrabutyl ammonium fluoride; nitric acid; sodium; phosphorus tribromide; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform; toluene; acetonitrile;
DOI:10.1039/c2cc35247h

Reference yield:

: 91668-84-7
2-bromo-6-methylpyridine N-oxide

: 1417729-48-6
C₆₄H₇₉N₅O₁₂P₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: nitric acid; sulfuric acid / 16 h / 0 - 100 °C

2.1: phosphorus tribromide / chloroform / 16 h / 60 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / toluene / 16 h / 125 °C / Inert atmosphere

4.1: Acetyl bromide / 16 h / 70 °C / Inert atmosphere

4.2: 0 °C

5.1: 72 h / 140 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 16 h / 65 °C / Inert atmosphere

7.1: 3 h / 120 °C

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; copper(l) iodide; tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere

9.1: ethanol; sodium / 50 °C / Inert atmosphere

10.1: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

11.1: potassium carbonate / acetonitrile / 1 h / 50 °C / Inert atmosphere

12.1: trifluoroacetic acid / dichloromethane / 0.5 h / 23 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Acetyl bromide; ethanol; sulfuric acid; tetrabutyl ammonium fluoride; nitric acid; sodium; phosphorus tribromide; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform; toluene; acetonitrile;
DOI:10.1039/c2cc35247h