C₃₁H₃₈O₁₀

Base Information

Chemical Name:C₃₁H₃₈O₁₀
CAS No.:266676-41-9
Molecular Formula:C₃₁H₃₈O₁₀
Molecular Weight:570.637
Hs Code.:

C<sub>31</sub>H<sub>38</sub>O<sub>10</sub>

Synonyms:C₃₁H₃₈O₁₀

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Chemical Property of C₃₁H₃₈O₁₀

Chemical Property:

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Technology Process of C₃₁H₃₈O₁₀

There total 12 articles about C₃₁H₃₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 591-51-5
phenyllithium

: 266676-40-8
C₂₅H₃₂O₁₀

: 266676-41-9
C₃₁H₃₈O₁₀

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 11034-45-0
1β,2α,9α,10β-tetrahydroxy-5α-cinnamoyloxytaxa-4(20),11-dien-13-one

: 266676-41-9
C₃₁H₃₈O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1: 73 percent / CuSO₄

2: 92 percent / pyridine / CH₂Cl₂ / 0 °C

3: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

4: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

5: 95 percent / imidazole / dimethylformamide / 20 °C

6: 81 percent / pyridine

7: TBAF / tetrahydrofuran

8: Bu₄N⁺AcO^- / butan-2-one / Heating

9: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

10: 76 percent / DMAP / 0 - 20 °C

11: 84 percent / tetrahydrofuran / -78 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; butanone; 1: ketalization / 2: cyclocondensation / 3: Hydrolysis / 4: dihydroxylation / 5: silylation / 6: mesylation / 7: desilylation / 8: Cyclization / 9: deketalization / 10: Acetylation / 11: Addition;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 13452-36-3
2,9,10-triacetyl-5-O-cinnamoyltaxicin-I

: 266676-41-9
C₃₁H₃₈O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1: 86 percent / NaOCH₃ / methanol; CH₂Cl₂ / 0 °C

2: 73 percent / CuSO₄

3: 92 percent / pyridine / CH₂Cl₂ / 0 °C

4: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

5: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

6: 95 percent / imidazole / dimethylformamide / 20 °C

7: 81 percent / pyridine

8: TBAF / tetrahydrofuran

9: Bu₄N⁺AcO^- / butan-2-one / Heating

10: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

11: 76 percent / DMAP / 0 - 20 °C

12: 84 percent / tetrahydrofuran / -78 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium methylate; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; butanone; 1: Deacetylation / 2: ketalization / 3: cyclocondensation / 4: Hydrolysis / 5: dihydroxylation / 6: silylation / 7: mesylation / 8: desilylation / 9: Cyclization / 10: deketalization / 11: Acetylation / 12: Addition;
DOI:10.1016/S0960-894X(00)00031-7