2-Aminobut-2-enediamide

Base Information

• Chemical Name: 2-Aminobut-2-enediamide
• CAS No.: 18486-76-5
• Molecular Formula: C₄H₇N₃O₂
• Molecular Weight: 129.118
• Hs Code.: 2924199090
• DSSTox Substance ID: DTXSID50695905
• Mol file: 18486-76-5.mol

Synonyms:2-AMINOBUT-2-ENEDIAMIDE;2-Aminobutenedioic Acid Diamide;DTXSID50695905;AKOS030255971;FT-0661623

Chemical Property of 2-Aminobut-2-enediamide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 185-190 °C
• Refractive Index: 1.583
• Boiling Point: 491.151°C at 760 mmHg
• PKA: 13.54±0.50(Predicted)
• Flash Point: 250.839°C
• PSA: 112.20000
• Density: 1.385g/cm³
• LogP: -0.09950
• Storage Temp.: Refrigerator
• Solubility.: DMSO
• XLogP3: -1.7
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 129.053826475
• Heavy Atom Count: 9
• Complexity: 173

Purity/Quality:

98%Min ^*data from raw suppliers

2-Amino-2-butenediamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=C(C(=O)N)N)C(=O)N

Technology Process of 2-Aminobut-2-enediamide

There total 5 articles about 2-Aminobut-2-enediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

1,1,1-Trimethyl-2-<1,2-bis(carbamoyl)ethyl>hydrazinium Iodide (88419-32-3) → 2-Aminobutenedioic Acid Diamide (18486-76-5)

Guidance literature:

With IRA-400 anion exchange resin; In water; passed through a column with resin;

DOI:10.1007/BF00506885

Reference yield:

→ 2-Aminobutenedioic Acid Diamide (18486-76-5)

Guidance literature:

With ammonium hydroxide; amino-butenedioic acid diamide, high-melting form; Kuehlung;

DOI:10.1001/jama.286.17.2092

Reference yield:

(Z)-2-chloro-2-butenedioic acid, diethyl ester (10302-94-0) → 2-Aminobutenedioic Acid Diamide (18486-76-5)

Guidance literature:

at 25 ℃;

upstream raw materials:

1,1,1-Trimethyl-2-<1,2-bis(carbamoyl)ethyl>hydrazinium Iodide

(Z)-2-chloro-2-butenedioic acid, diethyl ester

Refernces