C₂₆H₃₀N₂O₂S₂

Base Information

Chemical Name:C₂₆H₃₀N₂O₂S₂
CAS No.:1448802-17-2
Molecular Formula:C₂₆H₃₀N₂O₂S₂
Molecular Weight:466.668
Hs Code.:

C<sub>26</sub>H<sub>30</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:C₂₆H₃₀N₂O₂S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₀N₂O₂S₂

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Technology Process of C₂₆H₃₀N₂O₂S₂

There total 8 articles about C₂₆H₃₀N₂O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 540-63-6
ethane-1,2-dithiol

: 1448802-17-2
C₂₆H₃₀N₂O₂S₂

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₄H₂₆N₂O₃

: 1448802-17-2
C₂₆H₃₀N₂O₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1: Daicel Chiral-Pak AS / ethanol; hexane; diethylamine / Resolution of racemate

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; In ethanol; hexane; dichloromethane; diethylamine;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₆H₂₈N₂O₅

: 1448802-17-2
C₂₆H₃₀N₂O₂S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.28 h / 0 - 20 °C

1.2: 0.5 h

1.3: 0.5 h

2.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1 h / 110 °C

3.1: lithium hydroxide monohydrate / methanol; tetrahydrofuran; water / 50 °C

4.1: triethylamine; diphenyl phosphoryl azide / toluene; acetonitrile / 1.5 h / 30 °C

4.2: 2 h / 120 °C

5.1: triethylamine; lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

6.1: trimethyl(benzyl)ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

7.1: diethylamine / ethanol; hexane / Resolution of racemate

8.1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C

With lithium hydroxide monohydrate; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; trimethyl(benzyl)ammonium fluoride; sodium hydride; diethylamine; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; toluene; acetonitrile; mineral oil;
DOI:10.1002/chem.201604647