3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE

Base Information

Chemical Name:3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE
CAS No.:381194-08-7
Molecular Formula:C₁₅H₁₂BrN₃OS
Molecular Weight:362.25
Hs Code.:
Mol file:381194-08-7.mol

Synonyms:5-(4-bromophenoxymethyl)-4-phenyl-4H[1,2,4]triazole-3-thiol

Suppliers and Price of 3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE

Chemical Property:

Melting Point:211-213 °C(Solv: methanol (67-56-1))
Boiling Point:458.9±51.0 °C(Predicted)
PKA:4.80±0.20(Predicted)
Density:1.53±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE

There total 5 articles about 3-((4-BROMOPHENOXY)METHYL)-4-PHENYL-1,2,4-TRIAZOLINE-5-THIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 406190-67-8
C₁₅H₁₄BrN₃O₂S

: 381194-08-7
5-(4-bromophenoxymethyl)-4-phenyl-4H[1,2,4]triazole-3-thiol

Guidance literature:: With sodium hydroxide; for 1h; Reflux;
DOI:10.1021/jm3013213

Reference yield:

: 6964-29-0
ethyl 2-(4-bromophenoxy)acetate

: 381194-08-7
5-(4-bromophenoxymethyl)-4-phenyl-4H[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: ethanol / 1 h / Reflux

3: sodium hydroxide / 1 h / Reflux

With hydrazine hydrate; sodium hydroxide; In ethanol;
DOI:10.1021/jm3013213

Reference yield:

: 1878-91-7
(4-bromophenoxy)acetic acid

: 381194-08-7
5-(4-bromophenoxymethyl)-4-phenyl-4H[1,2,4]triazole-3-thiol

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / 3 h / Reflux

2: hydrazine hydrate / ethanol / 3 h / Reflux

3: ethanol / 1 h / Reflux

4: sodium hydroxide / 1 h / Reflux

With toluene-4-sulfonic acid; hydrazine hydrate; sodium hydroxide; In ethanol;
DOI:10.1021/jm3013213