1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)

Base Information

• Chemical Name: 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)
• CAS No.: 1637480-20-6
• Molecular Formula: C₆₂H₆₀N₆O₈
• Molecular Weight: 1017.19
• Mol file: 1637480-20-6.mol

Synonyms:1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)

Chemical Property of 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)

There total 5 articles about 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

4-((4-octanoyloxyphenyl)azo)benzaldehyde (1332372-67-4) + 3-(4-aminobenzoyloxy)phenyl 4-aminobenzoate (142280-58-8) → 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate) (1637480-20-6)

Guidance literature:

With acetic acid; In ethanol; for 2h; Reflux;

DOI:10.5562/cca2150

Reference yield:

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate (187264-29-5) → 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate) (1637480-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethanol / 6 h / Reflux

2: acetic acid / ethanol / 2 h / Reflux

With tin(II) chloride dihdyrate; acetic acid; In ethanol;

DOI:10.5562/cca2150

Reference yield:

recorcinol (108-46-3) → 1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate) (1637480-20-6)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: tin(II) chloride dihdyrate / ethanol / 6 h / Reflux

3: acetic acid / ethanol / 2 h / Reflux

With dmap; tin(II) chloride dihdyrate; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;

DOI:10.5562/cca2150

upstream raw materials:

4-((4-octanoyloxyphenyl)azo)benzaldehyde

3-(4-aminobenzoyloxy)phenyl 4-aminobenzoate

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate

recorcinol