[3-(4-Aminobenzoyl)oxyphenyl] 4-aminobenzoate

Base Information

• Chemical Name: [3-(4-Aminobenzoyl)oxyphenyl] 4-aminobenzoate
• CAS No.: 142280-58-8
• Molecular Formula: C₂₀H₁₆N₂O₄
• Molecular Weight: 348.358
• DSSTox Substance ID: DTXSID80897132
• Nikkaji Number: J814.845G
• Wikidata: Q81987967
• Mol file: 142280-58-8.mol

Synonyms:142280-58-8;CBDivE_013435;[3-(4-aminobenzoyl)oxyphenyl] 4-aminobenzoate;SCHEMBL107413;DTXSID80897132;1,3-bis(4-aminobenzoyloxy)benzene;1,3-Phenylene bis(4-aminobenzoate);CCG-327742;Bis(4-aminobenzoic acid)1,3-phenylene ester

Chemical Property of [3-(4-Aminobenzoyl)oxyphenyl] 4-aminobenzoate

Chemical Property:

• XLogP3: 3.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 6
• Exact Mass: 348.11100700
• Heavy Atom Count: 26
• Complexity: 440

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)OC(=O)C2=CC=C(C=C2)N)OC(=O)C3=CC=C(C=C3)N

Technology Process of [3-(4-Aminobenzoyl)oxyphenyl] 4-aminobenzoate

There total 5 articles about [3-(4-Aminobenzoyl)oxyphenyl] 4-aminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate (187264-29-5) → 3-(4-aminobenzoyloxy)phenyl 4-aminobenzoate (142280-58-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 6h; under 775.722 Torr;

DOI:10.1039/b100022p

Reference yield:

4-nitro-benzoyl chloride (122-04-3) → 3-(4-aminobenzoyloxy)phenyl 4-aminobenzoate (142280-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / pyridine / tetrahydrofuran / 24 h / 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 6 h / 775.72 Torr

With pyridine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;

DOI:10.1039/b100022p

Reference yield:

recorcinol (108-46-3) → 3-(4-aminobenzoyloxy)phenyl 4-aminobenzoate (142280-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / pyridine / tetrahydrofuran / 24 h / 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 6 h / 775.72 Torr

With pyridine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;

DOI:10.1039/b100022p

upstream raw materials:

3-(4-nitrobenzoyloxy)phenyl 4-nitrobenzoate

4-aminobenzoyl chloride

recorcinol

4-nitro-benzoyl chloride

Downstream raw materials:

1,3-phenylene bis(4-(4-((4-hexanoyloxyphenyl)azo)benzylideneamino)benzoate)

1,3-phenylene bis(4-(4-((4-heptanoyloxyphenyl)azo)benzylideneamino)benzoate)

1,3-phenylene bis(4-(4-((4-octanoyloxyphenyl)azo)benzylideneamino)benzoate)

1,3-phenylene bis(4-(4-((4-nonanoyloxyphenyl)azo)benzylideneamino)benzoate)