2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol

Base Information

• Chemical Name: 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol
• CAS No.: 863309-60-8
• Molecular Formula: C₂₂H₂₄Cl₂N₄O₂S₂
• Molecular Weight: 511.496

Synonyms:2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol

Chemical Property of 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol

There total 2 articles about 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

6-(2-piperidinothiazol-5-yl)-3,4,7-trichloro-2,5-dihydroxy-2,3-dihydrobenzo[b]furan hydrochloride + piperidine-1-carbothioamide (14294-09-8) → 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol (863309-60-8)

Guidance literature:

In ethanol; Heating;

DOI:10.3987/COM-05-10369

Reference yield:

2,3,5-trichloro-6-(2-piperidin-1-yl-thiazol-5-yl)-[1,4]benzoquinone → 2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol (863309-60-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / magnesium sulfate / toluene / 0.5 h / 20 °C

2: conc. HCl / acetonitrile / 1.5 h / Heating

With hydrogenchloride; magnesium sulfate; In toluene; acetonitrile;

DOI:10.1007/BF02297684

Reference yield: 74.0%

2,5-dichloro-3,6-bis-(2-piperidin-1-yl-thiazol-5-yl)-benzene-1,4-diol (863309-60-8) → 2,5-bis(2-piperidinothiazol-5-yl)-3,6-dichloro-1,4-benzoquinone

Guidance literature:

With iron(III) chloride; In water; N,N-dimethyl-formamide;

DOI:10.3987/COM-05-10369

upstream raw materials:

piperidine-1-carbothioamide

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