1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Base Information

Chemical Name:1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose
CAS No.:556054-09-2
Molecular Formula:C₄₇H₅₀O₉S
Molecular Weight:790.975
Hs Code.:

Synonyms:1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Suppliers and Price of 1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

There total 3 articles about 1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R,3S,4R,5R)-3-[(R)-Hydroxy-((2S,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-methyl]-4-phenylsulfanyl-6,8-dioxa-bicyclo[3.2.1]octan-2-one

: 556054-09-2
1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 0 ℃; for 2h;
DOI:10.1002/hlca.200390037

Reference yield:

: 108-98-5
thiophenol

: 556054-09-2
1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

2: 574 mg / NaBH₄ / methanol; CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/hlca.200390037

Reference yield:

: 270923-04-1
1,6-anhydro-3-C-[(1S)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-β-D-glycero-hex-2-en-4-ulopyranose

: 556054-09-2
1,6-anhydro-3-C-[(1R)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol-1-C-yl]-2,3-dideoxy-2-(phenylthio)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

2: 574 mg / NaBH₄ / methanol; CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/hlca.200390037